Photoreaction is a reaction which starts with light energy. It has a unique characteristic to give some product materials which are not the same as that of thermal reaction. Please refer to our technologies and facilities of photoreaction.
Photoreaction
Photoreaction is a reaction which starts with light energy. It has a unique characteristic to give some product materials which are not the same as that of thermal reaction.
High-pressure mercury-vapor lump is used as a light source and the temperature is controlled by water-cooling.
We possess several facilities with 8kW light source in Harima plant and each facility is able to perform the reaction of tens liters.
In addition, lab-scale synthesis can be performed with 100W and 400W of high-pressure mercury-vapor lumps at the chemical laboratory.
Further, we have performed flow reaction with FEP tube as well as general batch reaction.
Facilities
1. Production facilities (Harima plant)
・Light source : 8kW high-pressure mercury-vapor lump
・Filter : PYREX ®
・Stirring system : non-active gas bubbling, reaction liquid circulation
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2. Lab-scale (Chemical laboratory)
・Light source : 100/400W high-pressure mercury-vapor lump
・Filter : PYREX ®, quartz
・Stirring system : non-active gas bubbling, magnetic stirring
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3. Flow reactor (Chemical laboratory)
・Light source : 400W high-pressure mercury-vapor lump
・Filter : PYREX ®, quartz
・Channel : FEP tube (inner diameter: up to 1.2mm)
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Reaction example
[2+2] Photocyclization
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Vitamin D3
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Benzopinacol
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We are able to perform various synthesis with photoreaction.